NMR and Chemistry: An introduction to modern NMR spectroscopy, Fourth Edition

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CRC Press, 17 февр. 2000 г. - Всего страниц: 400
Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain.

The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.
 

Содержание

nuclear screening
17
Internuclear spinspin coupling
45
Nuclear magnetic relaxation
101
The spectrometer
129
Making the spins dance
167
NMR spectra of exchanging and reacting systems
189
Multiple resonance and onedimensional pulse sequences
233
Twodimensional NMR spectroscopy
273
Magnetic resonance imaging and biomedical NMR
335
Highresolution solidstate NMR
355
Bibliography
385
Answers to Questions
391
Index
397
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Advances in Sonochemistry, Том 4
T.J. Mason
Ограниченный просмотр - 1996

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